INDIUM(III) CHLORIDE HYDRATE
Indium chloride
CAS: 10025-82-8;12672-70-7
Molecular Formula: Cl3In
INDIUM(III) CHLORIDE HYDRATE - Names and Identifiers
| Name | Indium chloride |
| Synonyms | InCl3 Indium chloride INDIUM CHLORIDE Indium(Ⅲ)chloride Indium trichloride Indium(III) chloride indiumchloride(incl3) trichloroindium hydrate Indium chloride (InCl3) Indium trichloride anhydrous Indium(III) chloride hydrate IndiumchlorideanhydrousPURATREM Indium(III) chloride, synthesis grade Indium(III) chloride, anhydrous (metals basis) |
| CAS | 10025-82-8 12672-70-7 |
| EINECS | 233-043-0 |
| InChI | InChI=1/3ClH.In.H2O/h3*1H;;1H2/q;;;+3;/p-3 |
| InChIKey | PSCMQHVBLHHWTO-UHFFFAOYSA-K |
INDIUM(III) CHLORIDE HYDRATE - Physico-chemical Properties
| Molecular Formula | Cl3In |
| Molar Mass | 221.18 |
| Density | 3.46g/mLat 25°C(lit.) |
| Melting Point | 262°C (dec.)(lit.) |
| Boling Point | 300°C |
| Flash Point | 300°C subl. |
| Water Solubility | reacts |
| Vapor Presure | 1Pa at 25℃ |
| Appearance | White crystalline powder |
| Specific Gravity | 3.46 |
| Color | White to off-white |
| Exposure Limit | ACGIH: TWA 0.1 mg/m3NIOSH: TWA 0.1 mg/m3 |
| Merck | 14,4958 |
| Storage Condition | Inert atmosphere,Room Temperature |
| Stability | hygroscopic |
| Sensitive | Hygroscopic |
| MDL | MFCD00149744 |
| Physical and Chemical Properties | Melting point 586°C water-soluble reactions |
| Use | Used as a spectral purity and high purity reagent |
INDIUM(III) CHLORIDE HYDRATE - Risk and Safety
| Hazard Symbols | C - Corrosive |
| Risk Codes | R36/37/38 - Irritating to eyes, respiratory system and skin. R34 - Causes burns R29 - Contact with water liberates toxic gas R22 - Harmful if swallowed |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) |
| UN IDs | UN 3260 8/PG 2 |
| WGK Germany | 3 |
| RTECS | NL1400000 |
| FLUKA BRAND F CODES | 3-10 |
| TSCA | Yes |
| HS Code | 28273990 |
| Hazard Class | 8 |
| Packing Group | III |
| Toxicity | MLD s.c. in rats: 10.2 mg/kg; MLD i.v. in rabbits: 0.64 mg/kg, McCord et al., J. Ind. Hyg. Toxicol. 24, 243 (1942) |
INDIUM(III) CHLORIDE HYDRATE - Introduction
Easily soluble in water, slightly soluble in ethanol and ether.
Last Update：2022-10-16 17:11:21
INDIUM(III) CHLORIDE HYDRATE - Reference Information
| LogP | 5.9 at 22℃ |
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| Properties | Indium chloride is a colorless crystal with deliquescence. It sublimates above 600°C and is easily soluble in water and hydrolyzes. It can crystallize from aqueous solution. Tetrahydrate and pentahydrate. Dissolved in liquid ammonia to become a chloramine coordination compound. |
| use | indium chloride is the basic raw material for the synthesis of organic indium series compounds, and can also be used as a catalyst for organic reactions. it is also widely used in organic synthesis and electronic industry. At present, high purity anhydrous indium chloride is mainly used in the production of LED core chips, which belongs to the cutting-edge technology field of energy-saving semiconductor electronic lighting, and is an irreplaceable core raw material for LED representing the cutting-edge lighting technology. used as spectral purity and high purity reagent scientific research reagent, biochemical research effective catalyst, used for C- C bond formation, aldehyde reaction and reduction in aqueous solution. An efficient, mild Lewis acid for organic synthesis. |
| preparation | a synthesis method of anhydrous indium chloride, the process steps are: first, pretreatment: take 25kg of 5N high purity indium metal, place it in a vacuum Shi Ying furnace, hold it in a Shi Ying container coated with graphite composite material, then vacuum it, and gradually raise the temperature to 700-1200 ℃ after the negative pressure is stable, keep the temperature and negative pressure conditions unchanged for one hour. After the pretreatment is completed, close the vacuum valve, pass into high-purity argon after cooling, and take out the metal indium seal for storage under the protection of argon. the second is vacuum chlorination: put 25kg of pretreated high-purity indium ingot into a vacuum reactor, and put it in a quartz container with graphite composite coating. after the vacuum reactor is sealed, vacuum is drawn, and then high-purity argon is connected to exhaust the remaining gas in the vacuum reactor. after the negative pressure is stabilized, the temperature of the vacuum furnace is gradually increased from 500 ℃ to 1100 ℃. after the metal indium is completely dissolved into liquid, a small amount of high-purity chlorine gas is slowly introduced, the flow rate of high purity chlorine gas is in the range of 15-50m3/h, and the flow rate is gradually increased to 50 m3/h after the reaction is gradually stable. The reaction speed is controlled by accurately adjusting the temperature, chlorine flow rate and the pressure in the furnace, stabilizing the parameters and keeping the parameters unchanged for about 4 hours. The reaction is complete. After the vacuum furnace is cooled, the anhydrous indium chloride crystals are separated and taken out under the protection of high purity inert gas. And sealed for preservation. The third is sublimation purification: put the anhydrous indium chloride crystal into a high-temperature quartz distiller, and put it in a quartz container with a graphite composite material coating, vacuumize and stabilize the negative pressure, and slowly raise the temperature to a certain temperature. After the temperature is stable, the anhydrous indium chloride gradually volatilizes and crystallizes in the condensation zone, and controls the pressure in the distiller. After about 8 hours, the anhydrous indium chloride is sublimated and crystallized, and it is taken out under the protection of argon after, sealed packaging qualified after testing. |
| solubility in water (g/100ml) | dissolution grams per 100ml of water at different temperatures (℃): 210g/10 ℃;212g/20 ℃ |
| category | toxic substances |
| toxicity classification | highly toxic |
| acute toxicity | abdominal cavity-rat LD50: 2.370 mg/kg; Abdominal cavity-mouse LD50: 9.5 mg/kg |
| flammability hazard characteristics | high heat produces toxic chloride smoke |
| storage and transportation characteristics | warehouse ventilation and low temperature drying |
| fire extinguishing agent | dry powder, foam, sand, carbon dioxide, mist water |
| occupational standard | TWA 0.1 mg (indium)/m3 |
| toxic substance data | information provided by: pubchem.ncbi.nlm.nih.gov (external link) |
Last Update：2024-04-10 22:29:15
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